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Offline Eubanks6  
#1 Posted : Tuesday, February 21, 2012 4:26:48 AM(UTC)
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"Hey everyone, ran my essential pro extractor series II for the first time the other day and got 92% out of it! Strong stuff right there, but sure is smooth, pretty much flavorless just a whole lotta burn going down. My question to anyone and everyone is, if I have 5 gallons mash at around 15-17% how much 'drinkable' liquor should I get? I know the whole fill a bunch of jars with 200-300ml of produce let it sit a day and then start in the middle and work outwards, I was just wondering how much I should get that's good to drink after one run? I've heard 1/10 of your mash will be drinkable, but just thought i'd ask.

Next, when do you stop the run? As long as my head temp stays around 172-180 should I let it go until nothing comes out? It's in full reflux mode, packed with copper mesh and all, so I assume leaving it until nothing comes out anymore would make sense since only certain alcohols evaporate at those temps? I will disregard what smells bad/ off taste but I also want to get as much out of the mash as I can and I plan on just stocking up on heads and tails and running them again later, that's why I want to know, to make sure i'm not wasting potential alcohol in my mash!"
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#2 Posted : Tuesday, February 21, 2012 11:08:22 AM(UTC)
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Well I stopped at 180 yesterday and got chewed out for wasting ethanol. Found out later it was prob still pumping out hundred proof when I quit kick kick. I heard 184 kicked around somewhere and somebody say it will turn milky when it gets to sucking water. Kindly let me know when you find out:) Here is a very handy link with a built in calculator to do the math for ya. Its the 2nd table from the top of the page. Might have to register over there to use it. http://homedistiller.org/dtw.htm
Offline div4gold  
#3 Posted : Tuesday, February 21, 2012 12:42:16 PM(UTC)
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Toward the end of a run I start checking the abv. When it gets down to around 70 proof I quit and collect a little while longer into a container that I pour back into the next run. I have never use temperature for a guideline on pot still mode. I guess if you are referring to a reflux operation my advise is kaput.
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#4 Posted : Tuesday, February 21, 2012 1:41:34 PM(UTC)
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Sounds highly plausibe for any application. Thanks. I am going to buy an alchy checker tomorrow..they finally got them in at the Brewmesiter Shoppe. Think I take back an unopened bag of sweet feed too. I got to reading the ingredient list and it was recleaned whole oats..corn chops (aka corncobs maybe?)..Soy Bean Meal and Mollases Products. Now who would want to drink something made out of that crap? He musta thunk I just fell off the turnip truck to buy something like that. I am going to start reading the labels and quit taking folks word on something like that. He claimed it was rage amongst the local shiners etc. Had the highest protein content ect. Now was that boy fibbing to me?
Offline Eubanks6  
#5 Posted : Wednesday, February 22, 2012 3:32:46 AM(UTC)
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I am running full reflux, so i thought temp would be a good indicator, but I for sure think I stopped way too soon. Even if I'm not going to drink what comes out towards the end I plan on collecting it anyways, setting it aside, and re distilling later. I stopped when I was still get 90%abv because I had collected so much and I don't know why I had it in my head you only get 1/10 of the mash into alochol, but that's what I thought. So I figured what I was getting wouldn't be good anymore. I'm going to run it tomorrow and let her go as long as she'll pump stuff out. As for temp. in general though, by adjusting water flow and hotplate temp. it will never go over 180 (assuming I'm paying attention) so I figure i'll just let it run between 170-180 until I'm not getting anything, mathematically that makes sense to me since only certain alcohols evaporate at that temp, eventually if I keep the temp correct I shouldn't be getting anything....right?
Offline Bayou-Ruler  
#6 Posted : Wednesday, February 22, 2012 3:50:01 AM(UTC)
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Originally Posted by: Eubanks6 Go to Quoted Post
I am running full reflux, so i thought temp would be a good indicator, but I for sure think I stopped way too soon. Even if I'm not going to drink what comes out towards the end I plan on collecting it anyways, setting it aside, and re distilling later. I stopped when I was still get 90%abv because I had collected so much and I don't know why I had it in my head you only get 1/10 of the mash into alochol, but that's what I thought. So I figured what I was getting wouldn't be good anymore. I'm going to run it tomorrow and let her go as long as she'll pump stuff out. As for temp. in general though, by adjusting water flow and hotplate temp. it will never go over 180 (assuming I'm paying attention) so I figure i'll just let it run between 170-180 until I'm not getting anything, mathematically that makes sense to me since only certain alcohols evaporate at that temp, eventually if I keep the temp correct I shouldn't be getting anything....right?


sounds like you have the cart a head of the horse so to speak. I suggest you step back and do some more research in order to gain a better understanding of the process. How much product you get depends on the %ABV of your wash/mash if you start out knowing that it will give you an idea of what to expect. A proofing parrot and a alcohol hydrometer will help you immensely too.

There is a really good resource here: http://homedistiller.org/distill/dtw
Bayou Ethanol
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www.bayouethanol.com
Offline Eubanks6  
#7 Posted : Wednesday, February 22, 2012 4:18:35 AM(UTC)
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I have a hydrometer and alcometer. My wash was 17%abv when I ran it, I frequently was testing the produce as I stored it in 200-300ml mason jars, I understand that and the process. My question, mostly, was if stuff is still coming out, irregardless if I'm going to drink it (which I obviously wouldn't drink the end stuff) should I keep running it just to stock up heads and tails to re-run again later?
Offline Bayou-Ruler  
#8 Posted : Wednesday, February 22, 2012 4:22:04 AM(UTC)
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"
Originally Posted by: Eubanks6 Go to Quoted Post
I have a hydrometer and alcometer. My wash was 17%abv when I ran it, I frequently was testing the produce as I stored it in 200-300ml mason jars, I understand that and the process. My question, mostly, was if stuff is still coming out, irregardless if I'm going to drink it (which I obviously wouldn't drink the end stuff) should I keep running it just to stock up heads and tails to re-run again later?


Yes sir that is exactly what you should do. I collect down to 30%ABV and save it until i have enough to re distill it."
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Offline Eubanks6  
#9 Posted : Wednesday, February 22, 2012 4:23:45 AM(UTC)
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thanks Bayou! That link actually did help, given some of the math formulas I think I can better figure out how much I 'should' expect and then go from there if it's still coming out and do the whole let it sit a day, start in the middle smelling and tasting while working outward to find my hearts. Thanks for the help.
Offline Bayou-Ruler  
#10 Posted : Wednesday, February 22, 2012 4:48:30 AM(UTC)
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Originally Posted by: Eubanks6 Go to Quoted Post
thanks Bayou! That link actually did help, given some of the math formulas I think I can better figure out how much I 'should' expect and then go from there if it's still coming out and do the whole let it sit a day, start in the middle smelling and tasting while working outward to find my hearts. Thanks for the help.


You are welcome, glad I was able to help you out."
Bayou Ethanol
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www.bayouethanol.com
Offline heeler  
#11 Posted : Thursday, February 23, 2012 3:42:11 AM(UTC)
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Just a note...I read where someone stated that I will let it run between certain temps and then when it stops producing i'll turn it off. Well the temp will infact continue to rise and lots of times continue to produce well past the temps you have preset in your mind. Forget that mindset of I'm only gonna collect at a certain temp. Really you miss alot of good hooch if you say I'm gonna turn it off at a certain temp. Remember, you can collect down into the tails -- or should I say UP into the tails (up into higher temps is where the tails live). As you continue the run the temp goes up and the proof goes down. Thats just the way it is -- laws of physics I guess.
Offline Eubanks6  
#12 Posted : Thursday, February 23, 2012 6:27:46 AM(UTC)
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makes sense heeler i'll keep that in mind while distilling today. I guess what I'm having trouble wrapping my mind around is that on the homedistillers site all the alcohols we want in our liquor evaporate between like 170-180 and by adjusting the hotplate/water flow I can keep the top of the column at the temp. so eventually shouldn't nothing come out? Or more likely will the temp. just jump up because there's no more alcohol in that temp. range available to evaporate off and that's why you're telling me to run into the tails just to not waste?
Offline heeler  
#13 Posted : Thursday, February 23, 2012 7:30:58 AM(UTC)
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The fellers on that site are the experts no dought in my mind, and if we were vaporizing JUST ethanol we could leave it at a certain temp between 170-180. BUT with all the temp ranges, WE KNOW WHATS MOSTLY coming off at a specific temp. --- no what i mean. If the water to ethanol ratio is not even so to say, it takes more heat to get the product we are after. Also every distillation unit works juuuust alittle bit differently. So where mine might sit at 178 for 3 hours before starting to climb yours might sit there for 6 hours. What if my wash is 8% and yours is 18% and each have different amounts of water to make a boiler fill, well I'm pretty sure it would take diff. temps to capture whats inside. After you've made 5-6 runs you'll see what I'm saying.
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#14 Posted : Thursday, February 23, 2012 3:22:35 PM(UTC)
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Ok on my first keeper run a few days back I tried to let it reflux for about forty five mins at 165. Is that too low for the refluxing cycle to make it work good? Is there a recommended temp for refluxing? Or perhaps a visual clue for when it has reached the optimal reflux temps and duration. I noticed when it got much above that temp it started wanting to spit out hooch. It coughed up a bunch anyway. Thanks.
Offline div4gold  
#15 Posted : Thursday, February 23, 2012 4:08:16 PM(UTC)
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"
Originally Posted by: bigwheel Go to Quoted Post
Ok on my first keeper run a few days back I tried to let it reflux for about forty five mins at 165. Is that too low for the refluxing cycle to make it work good? Is there a recommended temp for refluxing? Or perhaps a visual clue for when it has reached the optimal reflux temps and duration. I noticed when it got much above that temp it started wanting to spit out hooch. It coughed up a bunch anyway. Thanks.


I believe you reflux at around 180 degrees or so. If you are spitting or surging out of your condenser then you have a low spot in your coil that is filling up and then when a little pressure builds it will spit it out."
Offline heeler  
#16 Posted : Friday, February 24, 2012 8:38:04 AM(UTC)
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or -- you might have had too much mash in the boiler to start with and it was puking out the top. If you have a 5 gallon boiler you cant put 5 gallons in it because of course it will expand and - boil over or puke over. Again I'm just guessing but thats what it sounds like happened.
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#17 Posted : Saturday, February 25, 2012 4:30:14 AM(UTC)
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Well the boiler was only half full or less. It seemed to reflux fine in the 16o's and started production when I cut back on water to the column and hit 177 or so. Nearly sure had it been allowed to get to 180 it would have not done much refluxing.
Offline mr. x  
#18 Posted : Monday, March 05, 2012 6:56:57 PM(UTC)
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guess i shouldnt have run my whole batch at 195ishi was just aiming for under 200 i guess ill stick closer to the 170-180 area it still powerful and tasty and it was my first one got 2.5 gal off a 13 gal wash only shitty thing i never got a seperate fermentor so did it in my keg so you taste a bit of burnt yeast but it sells still
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#19 Posted : Tuesday, March 06, 2012 3:07:53 AM(UTC)
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Havent got brave enough to try fermenting in the boiler yet..lol. I will put that on the to do list for one of these days.
Offline mr. x  
#20 Posted : Tuesday, March 06, 2012 8:17:27 PM(UTC)
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i wouldnt big wheel i just diddnt have anything seperate tio do it in or i would have it burns the yeast to the bottom and give but flavor
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