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#1 Posted : Thursday, May 17, 2007 4:07:33 AM(UTC)
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Hi

I bought a 4 gallon pot still on ebay and did not receive yet - I am newbie and have lots of questions - My appreciation for any assistance

I am thinking about using a 5 gallon water cooler bottle to make wash and ferment - this ok?

I like rum but want to keep ferment clean and simple with minimal risk of methanol so thinking of just sugar and water mash - maybe add rum essence later - comments?

how much sugar and water and black label turbo yeast to put in for one run of the 4 gallon pot still.? how long before ready to distill - how do you tell?



I was hoping to put this potstill on my stovetop ,indoors, to heat up - I have a good exhaust hood over stove and near a window also - is this ok to do inside ? or do I have to go outside with electric hot plate or propane for safety?

filtering - want to use a brita at first - when to filter ? how many times?

What else am I missing ? any other comments or pointers are welcome and apprecited - THANKS
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#2 Posted : Thursday, May 17, 2007 5:11:28 AM(UTC)
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John:

Welcome to the hobby.

Most recipes and yeast packs are set up for 25 liter which is 6.5 gallons. A 5 gallon carboy will work for some things but my advice is to pop for a 8 gallon fermentation bucket and air lock.

A simple recipe for rum is 16 pounds of dark brown sugar and a jar of molasses and a pack of turbo and filtered water up to 7 gal. Put two gallons of warm water ,120 df, in your bucket, stir in the sugar and mollasses then top off with cold water. Let it sit for a week. I promise you it will turn out much better than a white sugar wash with essence. You don't have to worry about methanol if you toss out the first 50 ml. This will make a 7 gallon batch.

Now to reduce this to 4 gallons, hmmmm... you may want to run this as two batches. Your stove top will work fine for such a small still.

I've never used a Brita so I will leave that for others.

Cheers and good luck
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#3 Posted : Thursday, May 17, 2007 6:49:10 AM(UTC)
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John,welcome.
I wouldnt use the brita on anything but neutral vodka.It will take all the flavors out of anything else.You should get some brewhaus carbon,and use it insted because its alot cheeper.You may not need to carbon filter anyway.
Are you going to run that still on a gas stove?
If you do,you better make sure that theres no vapor leaks,and use a long collection line,to keep the booze far away from the stove.I have a friend that runs that way all the time,and he has a good vent on his stove.He also cracks a window in the kitchen,to get better ventilation.
Keep a fire extinqusher close by,and never leave it unattended.
Colect your distillate in small amounts so you will get good seperation.I use coronna beer bottles that I have numbered.That way you can taste each bottle,with a little water,and seperate the good,from the not so good.Its a good way to do it when you are starting out,because your nose,and taste buds are in training.Just be careful,and take your time,and you will do fine.
wineo
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#4 Posted : Thursday, May 17, 2007 7:51:14 AM(UTC)
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How would I test for vapor leaks?
If I decide to do outside what is best electric burner to use for 4 gallon pot still?
I am getting a little concerned about doing this in the house - should I be?

I am leaning towards outside also because I have a 3 year old son - I would have to do this when he was not home if doing inside

I am giving up on the filter idea as you said I don't want vodka.

Any rum makers who use Natural unbleached cane sugar crystals and Molasses Powder instead of brown sugar and liquid molasses? I am looking at a site called bulkfoods.com and pricing looks good on this

How long would it take to distill 4 gallon pot still ? - how much of the 4 gallon would be drinkable?
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#5 Posted : Thursday, May 17, 2007 8:21:11 AM(UTC)
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When you get the still,do a run with water,and push it real hard{lots of heat}.Check all your connections real good for steam leaking.It will clean it out too.It will also give you an idea of how everything works.Dont be too concerned if it doesnt condence the water very good.Alcohal is much easer to condence than water.
Theres no way I could tell You how long it will take to do a 4 gallon run.If you do it outside,use a propane turkey burner.Its a lot faster.Once you get things heated up good,you can turn down the heat alot.Its best to run it slow and low,once it heats up.I run mine in the basement,but i have a large vent fan,and a large hood.{3ft by 5ft}.It would take a long time to heat 4 gallons on a hot plate.Im just getting into making rum,so I will leave that for the rum guys.If your careful,you could run inside,if you have a good vent,but it would be better to do it outside,at least until you know what your doing,and know your rig.
wineo
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#6 Posted : Thursday, May 17, 2007 9:57:18 AM(UTC)
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John:

Skimp on the ingredients skimp on the taste. Sixteen lbs pure cane DARK brown sugar, not one where they add molasses to white sugar, and a jar of molasses should set you back less than $20 and will produce the kind of product you are looking for. Unbleached cane sugar and molasses powder will not give you the rich molasses body you are looking for in rum.

Just for the record I truly believe that corn sugar makes a much better netural than regular cane sugar as well. I figure if I'm going to go to all the trouble of making a batch I want the best results, and that comes with the best ingredients.

As far as heating it, use a hot plate and you won't have any problems, inside or out.

As far as output from 4 gallons? I do a seven gallon wash and usually end up with 3 1/2 to 4 quarts of uncut ,87%, rum. Cut down to 80 prooof gives me a couple of gallons of excellent white rum. You can do the math from there.

Cheers
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#7 Posted : Thursday, May 17, 2007 11:37:00 AM(UTC)
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I like rum but want to keep ferment clean and simple with minimal risk of methanol so thinking of just sugar and water mash - maybe add rum essence later - comments?

Methanol and the type of liquor you're making are not related.

All washes produce methanol, in addition to a number of other non-ethanol alcohols.

Collect the first 50ml in a bottle of it's own, then switch to a different jug for the rest. After the foreshots, I collect in 1-gallon glass jugs, which used to hold cheap wine.

All alcohols in your wash have different boiling points. Methanol and several other bad ones boil at a lower temp than ethanol, so they will the first ones out.

Methanol in your moonshine isn't going to hurt you. The percentage of it in a run is so low that you'd kill yourself from alcohol poisoning before you could drink enough methanol to do you any harm.

But Methanol and the other 'Foreshots' alcohols will cause hangovers, bad smell, and bad taste.

Carbon filtering is largely something you do to fix broken stuff. Making your cuts accurately, watching your temps and keeping the heat low will generally eliminate any need for filtering.

If you filter, with Brita, or anything else that filters effectively, it will remove all flavors. Use it on Neutral Spirits only, because sugar washes are cheapest and easiest, and that's what you'll wind up with anyway, if you filter corn or molasses, etc. spirits.

Easiest ,but not best, thing is to make a simple sugar wash and add Rum Essence.

You can make Real Rum more cheaply, though ,Essences aren't cheap, and the essences I've tried personally really don't cut the mustard taste-wise, either.
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#8 Posted : Thursday, May 17, 2007 12:07:00 PM(UTC)
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how much sugar and water and black label turbo yeast to put in for one run of the 4 gallon pot still.? how long before ready to distill - how do you tell?

The question is how much do you use for your fermenter.

You ferment in a fermenter, then transfer however much you want into the distiller kettle for each run. You may take two or three runs to distill a single wash.

You let it ferment until it quits bubbling and smelling like fresh-baked bread.

Also, you can taste a little, and if it still tastes sweet, it isn't finished.

Or, you can also check the alcohol content with one of the two hydrometers/alcoholometers you should have bought with your still. One is for testing high-strength alcohol, in the 50%-90% range, and the other is for testing washes, in the 6%-20% range.

I ferment in a spare bedroom, so the wash can stay in the air-conditioning, and it makes the whole house smell like we're baking bread. Too much heat during ferment kills the yeast. Too much cold extends the number of days it takes to finish fermenting.

Most packets of turbo yeast tell you how much water and sugar to use with that packet. Heat the water to dissolve the sugar into, then top it off with tap water or otherwise let it cool to room temp before adding yeast.

Generally it takes about a week to fully ferment, sometimes two weeks. Even Turbo-Pure 48 ,sold by Brewhaus, actually takes up to 7 days, if you want the full potential. It's only 48 hours if you will settle for lower starting alcohol percentage.
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#9 Posted : Thursday, May 17, 2007 12:37:00 PM(UTC)
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Posted by John Marino on Thursday, May 17, 2007 - 11:07 am:

I was hoping to put this potstill on my stovetop ,indoors, to heat up - I have a good exhaust hood over stove and near a window also - is this ok to do inside ? or do I have to go outside with electric hot plate or propane for safety?

The problem with an electric range or hotplate is that they use thermostats. You can't heat the element up to 600 degrees, then let it cool down to 400, then cycle up again to 600, over and over and that's what a thermostatic control does.

The biggest safety problem is if you are using an open flame.

You are extracting a liquid that's more volatile than gasoline. It's fumes, especially if created by spillage, can make a big fire in less than a heartbeat. There's not too much danger of that unless you're distilling in a closet, which could fill with fumes, or a collection-vessel gets spilled or overflows. You just keep at least a couple of feet between your collection vessel and your open flame, and be sure the output hose isn't leaking in between them.

Best to keep a large-ish fire extinguisher wherever you are heating a still with any open flame. I use Propane, outdoors, for safety and convenience. It gets the wash up to temp fast, then I can turn it WAY down for the rest of the run.

You can get a good outdoor propane burner for cheap at Academy Outdoors, I think they're about $18, and you can mail-order them.

If using a hotplate, you need to disable the hotplate's thermostat, then use a 'Router Speed Control' to provide constant but lower current. You can get one cheaply at www.harborfreight.com.

After you get your kettle up to boiling temp, you want to use as little heat as possible to keep it there. Too much heat will affect purity of the output.

A natural gas range will work as a heat source, if your still column is short enough to physically fit under the range hood. But keep in mind that you have to lift a kettle plus several gallons of liquid up onto the burner. And if an alcohol fire happens, it's right there in the house with you.
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#10 Posted : Thursday, May 17, 2007 10:49:01 PM(UTC)
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thanks for all the info
I got my still in mail - anybody deal with ethanolpro on ebay - I thought it would be bigger - did not measure yet but cannot beleive that 4 gallons will fit in pot, looks a little cheesy for $80 and also charge 28 for shipping ups - I am starting to feel ripped off already. please comment
THANKS AGAIN TO ALL
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#11 Posted : Friday, May 18, 2007 3:18:45 AM(UTC)
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All of those types of stills are pot still variations regardless of the claims. You can run a little over 3 gallons in that one, so two runs from one 25L wash. It will take a long time for a run compared to a 2 or 3 inch column, but you probably don't need much anyhow so in most cases its about right. His work isn't very fancy but its safe and effective. He doesn't do a boil out so run water and one wash and throw it all away, then start keeping on the second run. If you like the way that one works, you can get a very nice pot column from Rick and stick it on a small keg later on if you decide to upgrade. Listen to these folks , they know what they are doing and have gone through all the trial and error so they can save you some grief.
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#12 Posted : Friday, May 18, 2007 3:54:02 AM(UTC)
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Thanks Brew - I was planning to do a water only run first but did not plan for discarding a wash run - is this for taste or safety? I bought a starter kit here so my first wash will have enough for 2 still runs.

I did not get a good description on how the cooling process works - I received a small pump with the still but was told to keep the cooling pot higher up - confused about how this will work and how to set it up - guess I need to do more reading and start experimenting - I don;t need to cool on the water only run , right?
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#13 Posted : Friday, May 18, 2007 4:17:13 AM(UTC)
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You could probably keep the first wash, but if it was me I would see how everything works and toss it. Steam will clean most of the stuff, but anything thats left that will soak into ethanol should go as well.

Yes the cooling bucket must be lower than the put because the pump is too small to pump through and back up so gravity needs to be available to help take it back to the cooling bucket.

yes, cool on the water or you will get clouds of steam. don't gauge the water run as to how it will run with wash. Remember it though since you will want distilled water to cut with later.

What came on the CD?

every single machine is different and needs its own special touch. be patient while learning. Listen to these guys, read thier old posts.
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#14 Posted : Friday, May 18, 2007 6:17:14 AM(UTC)
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The CD is almost worthless - has alot of stuff copied off other websites - some recipes, etc. nothing that great as far as I can see - It does not even show the unit setup fully - just pictures of the parts - I wanted to see how it should look fully setup - I will copy the cd and send it to anyone who wants a copy - just let me know where to send

another dumb question: on the condensor the cool water in should go in the lower of the two inputs? and output from higher back into the cool water bucket? I wish seller would have included a picture of the fully assembled still

also if i wanted to extend the receiver so that collection takes place further away from the heat source, does it have to be copper pipe - does it get too hot to just clamp a hose on it?

THANKS
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#15 Posted : Friday, May 18, 2007 6:23:03 AM(UTC)
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anywhere I could see a picture of a pot still with cooling bucket all setup with hose connections and heights ??
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#16 Posted : Friday, May 18, 2007 7:46:27 AM(UTC)
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Yes cold bottom and out on top. always on every condenser like that.

Some people use long hoses and then the sink instead of a bucket. The guy that built and sold it should be answering these kinds of questions though.
Go to Homedistiller.com and start at the beginning and read for a couple days. all your questions will be answered.
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#17 Posted : Friday, May 18, 2007 8:05:26 AM(UTC)
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Hi
just figured out that the cd that came with my still is the download of homedistiller.org. will read it through and see

If anyone can tolerate another stupid question here it is
If i wanted to extend the receiver so that collection takes place further away from the heat source, does it have to be copper pipe - does it get too hot to just clamp a hose on it?
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#18 Posted : Friday, May 18, 2007 9:05:00 AM(UTC)
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At 10:54 AM 05/18/2007, you wrote:

I did not get a good description on how the cooling process works - I received a small pump with the still but was told to keep the cooling pot higher up - confused about how this will work and how to set it up - guess I need to do more reading and start experimenting - I don't need to cool on the water only run, right? ______________________________________________________________________________ You need to cool any time you're distilling, even if it's distilled water.

Otherwise, your condenser will eventually become the same temp as the steam, and probably melt your hoses. Also when the condenser is almost the same temp as the steam, nearly no condensing will happen, your output will be mostly steam.

Cooling can be problematic. Some people just run a couple of garden hoses, ,with adaptors, and water their lawns as a by-product of condensing. You don't need a huge water-flow, just enough to keep it moving.

I guess that works, but even at low flow, you'd be surprised how much water your faucet will dispense in five or six hours. Most people use a recycling scheme, where they buy a used 55-gallon barrel and pump water from the barrel,s, through the condenser, back into the barrel. I bought a used plastic 55-gallon barrel for $15.

Even at that, you'd be surprised how well you can heat 55 gallons of water just from cooling the steam in a little condenser. Often, a radiator is used.

I have a motorcycle radiator that I got on Ebay for about $40, delivered. Or you can get a transmission cooler from an auto parts store for about $100. Run your cooling water through it, with a fan blowing on the fins, and it will get the job done.

The cooler you keep the condenser, the more efficient it will be, but really, as soon as it's cool enough to not be shooting any steam from the output end, that's cool enough, and it doesn't take all that much.

If you just put three or four gallons a kitchen sink, and pump in/out of that sink, it might be enough. Most people who use small-capacity cooling sources also freeze water in several 2-liter soft-drink bottles or milk jugs, and drop those into their cooling water one-by-one at intervals during the run.
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#19 Posted : Friday, May 18, 2007 9:08:02 AM(UTC)
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No hoses. they will all melt into the distillate at some point. Contact Rick and ask about his chem tolerant hose and if it will perform for that.

No it should be about room temp or cooler coming out if the condenser was built right.
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#20 Posted : Friday, May 18, 2007 9:35:00 AM(UTC)
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At 01:17 PM 05/18/2007, you wrote: also if i wanted to extend the receiver so that collection takes place further away from the heat source, does it have to be copper pipe - does it get too hot to just clamp a hose on it? ________________________________________________________________________________ _ Unless you do a run with no cooling water, there should not be a problem with hoses or most flexible tubing standing the heat.

The main thing about the hose running from your condenser to your collection vessel is that it be impervious to high-strength alcohol.

If the alcohol dissolves it, you'll be drinking it, in addition to the hose eventually getting brittle and breaking, possibly during a run. ,Alcohol Fire?,

Copper would add a little extra cooling, and might improve the flavor of the product if your system has no copper in it already. It's good to have some copper in the vapor-path, but I don't know if there would be any benefit in exposing already-condensed output to it.
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