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Offline Tea Totaler  
#1 Posted : Monday, August 06, 2012 12:58:55 PM(UTC)
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"I got my efficient stove built, had my PS2Hi Cap all vinegared out and packed with copper, and 5 gallons of what might be a pretty good first ferment. I upgraded my thermometer to a wireless remote gizmo designed for the grill. ( get one!)

Set the whole thing up with a big marine cooler full of water and three 1 gallon ice jugs for coolant. Fired the burner and got a case of mason jars ready. Cranked up the heat...really put it to her until I heard the first rumblings from the pot then turned the heat way down. Column was still cool. Turned on condensor coolant only. Head temp had not yet moved.

Felt the column to keep track of the vapor location as she rose. When the first drips came down the pipe, I just cracked the valve on the reflux and dropped the head temp down to 80 degrees immediately. then I waited...

Temp lowly rose to 170 and it started dripping. Came up to 176 and stayed there with a little stream broken occasionally into drips. Head temp bumped up two degrees about halfway through and I cracked the reflux a little bit more. Realized my coolant tank had warmed to maybe a hundred degrees so I refreshed it with hose water. Stayed like this for a long time until flow started to slow down a lot. Turned up the fire a little and opened the reflux a little. Temperature didn't move, but flow resumed.

I babied it through the last until the flow stopped completely and the head temp got up to 180 and stopped. I stopped the reflux and collected the tails of less than a pint. The head temp went up to 212 and I turned off the fire

Collecting, I ran the first half pint into a seperate jar, mostly to have some fore shots to learn what they smell like (what the hell is that? Acetone and ether? It smells like it would strip varnish). Then I collected another pint that smelled like ""cheap tequila"". Then I collected everything in my test cylinder to monitor ABV. Three quarts of perfectly clear ETOH that all floated between 92 and 94% (not proof). The last cylinder before it stopped was 86%. The tails without reflux was 20% and smells of burnt wine. Just shy of a gallon of fuel over 180 proof with 3 quarts comestible. About 3.5 hours including warm up and changing out a propane cylinder.

My impression is that the fire controls how much vapor is available and the reflux head controls the temperature of the vapor allowed through to the condenser? The more vapor available, the more reflux needed to keep the temp down. If so, it is a lot simpler to run a reflux rig than I was led to believe."
Offline Farmin in the woods  
#2 Posted : Monday, August 13, 2012 4:16:24 PM(UTC)
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Tea, congrats on your first run, I believe the fore's are a mix of acetone and wood alcohol, and smell like fingernail polish remover. I save mine for parts cleaner, degreaser, etc. BTW, thats a nice ABV you got there, I think my best has been high 80's. Also your getting a really good volume, mine averages a pint of 170ish proof per gallon of mash, which translates into almost 5 quarts of 90 proof per 5 gallon run.

I've noticed if you keep the heat high you end up with product that has a lot of burn and not a desirable taste, so I try to keep the heat after bringing to temp at a low setting. Also if your water gets too hot the same thing happens. I started with a cooler and upgraded to a 55 gallon barrel and 3 liter bottles of frozen water to cool.

I use a turkey fryer burner and it comes to temp pretty quick, around 30 mins on a 5 gallon mash/wash.
Hope this helps

Farmin
Offline cczero  
#3 Posted : Tuesday, August 14, 2012 1:14:51 AM(UTC)
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Originally Posted by: Tea Totaler Go to Quoted Post
About 3.5 hours including warm up and changing out a propane cylinder.


I'm a little confused here. It sounds like you're doing a reflux run using both columns packed? But the time 3.5 hours sounds like a striping run. My striping runs (I have 6 under my belt) usually run around 3 hrs drawing about 5 qts. 1st qt is in the 60 ABV and declines from there, to around 30 ABV when I stop the run. My last spirit, REFLUX, run (3.5 gals) was a little over 12 hours with ABV in the 90's for the 1st 4 qts, then dropping to 85 ABV for the 5th qt. I've been using BW sugar wash using EC 1118 yeast. I use 2 pumps from 2 55 gals barrels when doing REFLUX, but 1 pump from 1 barrel for the striping run. The reading I've done on this forum suggests a FAST striping(s) run then a slow spirit (reflux) run. Am I missing something??????

Regards to all.
Offline John Barleycorn  
#4 Posted : Tuesday, August 14, 2012 2:01:21 AM(UTC)
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"
Originally Posted by: cczero Go to Quoted Post
It sounds like you're doing a reflux run using both columns packed? But the time 3.5 hours sounds like a striping run.
I pack the entire column including some extra mesh stuffed around the cooling tubes. The time sounds right for ""a little stream broken occasionally into drips.""

Originally Posted by: cczero Go to Quoted Post
The reading I've done on this forum suggests a FAST striping(s) run then a slow spirit (reflux) run. Am I missing something??????
Nope. You're not missing something ... you're spot on.


CC: It sounds like you're getting some nice results WRT abv and volume. Congrats!


Tea: Are you making fuel?

--JB"
Offline Farmin in the woods  
#5 Posted : Tuesday, August 14, 2012 5:44:45 PM(UTC)
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QUOTE=cczero;17179]I'm a little confused here. It sounds like you're doing a reflux run using both columns packed? But the time 3.5 hours sounds like a striping run. My striping runs (I have 6 under my belt) usually run around 3 hrs drawing about 5 qts. 1st qt is in the 60 ABV and declines from there, to around 30 ABV when I stop the run. My last spirit, REFLUX, run (3.5 gals) was a little over 12 hours with ABV in the 90's for the 1st 4 qts, then dropping to 85 ABV for the 5th qt. I've been using BW sugar wash using EC 1118 yeast. I use 2 pumps from 2 55 gals barrels when doing REFLUX, but 1 pump from 1 barrel for the striping run. The reading I've done on this forum suggests a FAST striping(s) run then a slow spirit (reflux) run. Am I missing something??????

Regards to all.



Ok, its my turn to be confused. CC and JB, I usually run a 5 gallon wash in reflux with both columns packed using propane for heat and it takes about 30 minutes everytime to bring it to temp, then I back the heat way down and get a small stream w/ a few drips and collect 4 to 5 pints. The first few (3 or 4) pint runs right at 15 minutes each, sometimes a little faster for the first one, but average 15 minutes. Then the last 1 or 2 take a little longer, like 20 to 30 minutes. Then it slows to a drop every 2 to 3 seconds and I shut it down. I just averaged the last pint of all my runs and the average ABV of the last pint is 136 proof. This all takes a little over 2 hours.

CC, you said your stripping run takes you about 3 hours and your spirit run takes you 12 hours, correct? Is that for a 5 gallon wash? Are you using gas or hot plate for heat?

I guess the $64,000 question is am I running my still too fast? The neutral run gives me a smooth product almost everyone likes. I've tried turning down the heat further, but the stream turns to a trickle and I dont notice a difference in taste.

I'm not knocking what you are doing, I'm trying to figure out if I'm doing this right. I've only done 14 runs thus far, so I'm far from a expert.

Farmin
Offline Farmin in the woods  
#6 Posted : Tuesday, August 14, 2012 5:46:10 PM(UTC)
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Originally Posted by: cczero Go to Quoted Post
I'm a little confused here. It sounds like you're doing a reflux run using both columns packed? But the time 3.5 hours sounds like a striping run. My striping runs (I have 6 under my belt) usually run around 3 hrs drawing about 5 qts. 1st qt is in the 60 ABV and declines from there, to around 30 ABV when I stop the run. My last spirit, REFLUX, run (3.5 gals) was a little over 12 hours with ABV in the 90's for the 1st 4 qts, then dropping to 85 ABV for the 5th qt. I've been using BW sugar wash using EC 1118 yeast. I use 2 pumps from 2 55 gals barrels when doing REFLUX, but 1 pump from 1 barrel for the striping run. The reading I've done on this forum suggests a FAST striping(s) run then a slow spirit (reflux) run. Am I missing something??????

Regards to all.




Ok, its my turn to be confused. CC and JB, I usually run a 5 gallon wash in reflux with both columns packed using propane for heat and it takes about 30 minutes everytime to bring it to temp, then I back the heat way down and get a small stream w/ a few drips and collect 4 to 5 pints. The first few (3 or 4) pint runs right at 15 minutes each, sometimes a little faster for the first one, but average 15 minutes. Then the last 1 or 2 take a little longer, like 20 to 30 minutes. Then it slows to a drop every 2 to 3 seconds and I shut it down. I just averaged the last pint of all my runs and the average ABV of the last pint is 136 proof. This all takes a little over 2 hours.

CC, you said your stripping run takes you about 3 hours and your spirit run takes you 12 hours, correct? Is that for a 5 gallon wash? Are you using gas or hot plate for heat?

I guess the $64,000 question is am I running my still too fast? The neutral run gives me a smooth product almost everyone likes. I've tried turning down the heat further, but the stream turns to a trickle and I dont notice a difference in taste.

I'm not knocking what you are doing, I'm trying to figure out if I'm doing this right. I've only done 14 runs thus far, so I'm far from a expert.

Farmin
Offline johnnyapplepie  
#7 Posted : Wednesday, August 15, 2012 12:08:14 AM(UTC)
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Originally Posted by: Tea Totaler Go to Quoted Post
all vinegared out


Could you explain a bit more what this means "All Vinegar'd out"?

Thanks
Offline cczero  
#8 Posted : Wednesday, August 15, 2012 1:02:01 AM(UTC)
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"
Originally Posted by: Farmin in the woods Go to Quoted Post


CC, you said your stripping run takes you about 3 hours and your spirit run takes you 12 hours, correct? Is that for a 5 gallon wash? Are you using gas or hot plate for heat?

I guess the $64,000 question is am I running my still too fast? The neutral run gives me a smooth product almost everyone likes. I've tried turning down the heat further, but the stream turns to a trickle and I dont notice a difference in taste.

I'm not knocking what you are doing, I'm trying to figure out if I'm doing this right. I've only done 14 runs thus far, so I'm far from a expert.

Farmin


The striping runs I've done so far have been from 3 to 3+ hours. I'm using propane heat with a steel diffuser. Looking back over my spreadsheet the first jar (I decided to use quart jars for striping runs) comes off at about 1 1/2 hours into turning on the propane. That's after collecting and discarding 150 ml. This is only my second set of 3 striping runs so am still looking for advice and guidance. I used this basic procedure for all 3 striping runs and seemed to have worked out well. I used to use 1/2 pint, then 1 pint jars, but because everything will go thru a REFLUX run I decided to use quart jars this time. As the jars come off (32 oz) using paper coffee filters, I'll number the jar, write the temp range, eg, 174-175, and the ABV of that jar. Screw on the lid and set it aside. When the ABV drops to between 10 and 20 I stop the run by turning of the heat, pump and removing the rubber stopper.

I have been trying to speed up these runs but seems the temp get out of control. I imagine I'll eventually learn to use the heat and cooling to better advantage. Once I see a steady un-broken stream, I'll try to leave it there as long as I can. I've noticed on the last 3 runs the best output is between 174-180.

I've only used Birdwatchers sugar wash recipe for a 5 gal wash but because of raking and leaving head space, only about 4 1/2 gals make it to the boiler.

The time between jars is 15 - 40 minutes. Seems the last, 5th quart, takes the most time.

My REFLUX run, like I said is around 12 hours. I've only done a couple but have had good results by lowering the heat and collecting a drop every 1/2 to 1 second. My bottom column is packed completely, the top column only has 1 roll of copper at the intersection of the cooling tubes. Though I think for my next REFLUX run I'll fill up the upper column as well.

Maybe we're comparing apples to oranges here though. I'm talking about striping runs using just the upper tower of my PSII HC, while you're talking about REFLUXing using both columns. I'll combine all output, 15 quarts, and dilute to around 5 gals then start the REFLUX. My last REFLUX run produced 5 pints (here I use the smaller jars) of around 190 proof. I use the same procedure here, number the jars, record the temp range, and the ABV. I'm hoping, eventually, I'll be able to use these numbers to help make 'cuts'."
Offline texaswhitewolf  
#9 Posted : Wednesday, August 15, 2012 5:17:48 AM(UTC)
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ok i got a question who all use a reflux still and or pot still? my pot still takes me about 3 to 4 hours doing a stripping of 5 gals comes off at 135proof . spirit runs take about 3hrs for 3 gals of 50 abv. always come off at 165 proof during spirit runs
Offline cczero  
#10 Posted : Wednesday, August 15, 2012 6:00:36 AM(UTC)
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"
Originally Posted by: texaswhitewolf Go to Quoted Post
ok i got a question who all use a reflux still and a pot still? my pot still takes me about 3 to 4 hours doing a stripping of 5 gals comes off at 135proof . spirit runs take about 3hrs for 3 gals of 50 abv. always come off at 165 proof during spirit runs


Running about the same time but I'm not getting the proof you are. I did 3 striping runs over the past 4 days and average about 44 ABV over the 15 quarts I've saved for the reflux run. I'm hoping when I do the reflux run I'll get 90-95 ABV for several pints. I'm being convinced that I can speed up my reflux runs and see the same output as you.

Did you mean to say your reflux runs always come out at 165 proof, not spirit runs?"
Offline texaswhitewolf  
#11 Posted : Wednesday, August 15, 2012 6:36:32 AM(UTC)
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I dont use a reflux i got just a old school copper pot still. My stripping run is more like a spirit run i ride slow and low collect about 4-6 pints or till i hit about 40 to 30% abv. Save that up for about 4 runs then i throw it back in and do a spirit run. Thats the main reason im getting high proof on the stripping run.
Offline John Barleycorn  
#12 Posted : Wednesday, August 15, 2012 8:46:33 AM(UTC)
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"
Originally Posted by: Farmin in the woods Go to Quoted Post
I guess the $64,000 question is am I running my still too fast? The neutral run gives me a smooth product almost everyone likes.

Then I'd say you're doing it right. Don't let anyone tell you any different. If you're safe and having fun AND you like what you're making, then you're doing it right ... that's a good thing!

I'm no expert either, but I'm learning ... mostly from mistakes. IMO there's no substitute for hands on experience. I like running the machine and experimenting with stuff. That's where the fun is for me ... I tinker & fiddle around with things. Sometimes they work out, sometimes they don't. I'm really not much of a drinker ... I can take it or leave it ... and I'm not jockeying to be the home distiller of the year either. So any mistakes or failed experiments are no big deal. I'm just learning yet another way NOT to do things. Wink

Best Regards,
--JB"
Offline John Barleycorn  
#13 Posted : Wednesday, August 15, 2012 8:52:55 AM(UTC)
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Originally Posted by: Farmin in the woods Go to Quoted Post
which translates into almost 5 quarts of 90 proof per 5 gallon run.
BTW: That's very close to what I'll get from a stripping run. I'll throw two of those runs (diluted to about 40%) in for a spirit run and keep 1 L (maybe 1.5L on a really good run) at 93%.
Offline Farmin in the woods  
#14 Posted : Wednesday, August 15, 2012 6:09:15 PM(UTC)
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Originally Posted by: bigwheel Go to Quoted Post
My state of the art BH refluxer spits out 170 proof regardless of the machinations of mere mortals. It take 3-4 hrs and if somebody can figger out how to slow it down or speed it up..kindly give the scoop. Do it once..do it right..quit clowning around.


And THERE gentlemen are truly pearls of wisdom. Little did we know we were "clowning around". I notice this thread had gone about 12 post without someone pointing out the ills of our ways, I for one am SO glad BW has graced us with his presence, experience, and mostly, his point of view.

Farmin
Offline Tea Totaler  
#15 Posted : Monday, August 20, 2012 9:02:58 AM(UTC)
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"By ""vinegared out"" I mean I set up my still without packing and ran a couple of gallons of 50/50 vinegar/water through to clean it. Used cider vinegar and collected clear distillate, making sure everything worked.

I was running full reflux with as much copper packing as I could stuff in top and bottom, without any voids. I still could not detect resistance when breathing through the packing.

I did not do a stripping run as I had fermented to somewhere between 40 and 50 proof, Over 20% ABV.

I am making fuel, with a comestible coproduct. That is, making high purity ethanol that is drinkable, without regard to any kind of ""whiskey"". Just nuetral spirits that will burn and perhaps run a generator. My product ran a marine pressure stove very nicely.

As an update, 3 tasters all said that it had a yeasty taste or smell, symmetrical inebriation, and hangover no worse than expected. In the hindsight that comes with fermenting my second batch, I now know my wash was still actively fermenting when I put it in the still. Second run will be with a mature wash using the same yeast cake as the first. I will see if I can get rid of the yeasty smell.

Yes, 3.5 hours on full reflux. Temperature stable and fire real low. I only used high heat to bring it up to a rumble. I guess the ""equilibrium"" I have read about is that groove where the available vapor (heat) is right at the point where the reflux can easily knock it down.

Too fast? I got 3 quarts of drinkable (well, not poisonous) at over 180 (I collected it all in a test cylindar and took AG before putting it in the jar. All but the last 100ML were between 91 and 94%. The last 100ML cylinder was at 86%) and another pint and a half of poisonous but high test fuel. What might I have gotten if I slowed down?

My kettle was shiny clean inside when I was done, just rinsed it out with a hose."
Offline Fusefinder  
#16 Posted : Tuesday, August 21, 2012 3:54:02 AM(UTC)
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My last 2 REFLUX runs UJSM and All Brann fermented to 12.61% (5-6 gallon) and 12.26% (6 gallon) respectively each produced 6-7 pints starting at 93% staying there until the 4th or 5th ending at 85%. That's throwing out the first 1/2 pint to pint of fores and heads, and a pint of tails.
It takes me about 30 minutes to heat, 1 hour of refluxing (no dripping or stream) then about 3 hours of fast drip but not stream. Then 1/2 hour to clean up.
I have 4 rolls copper in each section of PSII HC . An 8 gallon kettle with internal heater. I use 1 pump from a 15 gallon cooler filled with 54 deg well water. I use 2-3 coolers of water. When its luke warm I water the plants and refill.
I get a clean neutral to slight corn/wheat taste. I don't have to carbon filter, unless I get some early tails I decide to keep.
Offline scotty  
#17 Posted : Tuesday, August 21, 2012 4:11:43 AM(UTC)
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FF--- Are you saying that your washes measures at 12+% and 12+% potential alcohol???:)
Offline Fusefinder  
#18 Posted : Tuesday, August 21, 2012 4:12:23 AM(UTC)
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"
Originally Posted by: John Barleycorn Go to Quoted Post
Then I'd say you're doing it right. Don't let anyone tell you any different. If you're safe and having fun AND you like what you're making, then you're doing it right ... that's a good thing!

I'm no expert either, but I'm learning ... mostly from mistakes. IMO there's no substitute for hands on experience. I like running the machine and experimenting with stuff. That's where the fun is for me ... I tinker & fiddle around with things. Sometimes they work out, sometimes they don't. I'm really not much of a drinker ... I can take it or leave it ... and I'm not jockeying to be the home distiller of the year either. So any mistakes or failed experiments are no big deal. I'm just learning yet another way NOT to do things. Wink

Best Regards,
--JB


I agree, its also reassuring to know that you are on the same page as many others with a similar setup! Cool"
Offline Fusefinder  
#19 Posted : Tuesday, August 21, 2012 7:57:56 AM(UTC)
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"
Originally Posted by: scotty Go to Quoted Post
FF--- Are you saying that your washes measures at 12+% and 12+% potential alcohol???:)


Starting Gravity = 1.078
Final Gravity = 0.98
(Start-final)*129= % potential (1.078-0.98)*129=12.64%
I assume the formula and math is correct??
I created an excell formula/Brew log baed on http://homedistiller.org...cs/alcohol_content"
Offline Fusefinder  
#20 Posted : Tuesday, August 21, 2012 8:07:31 AM(UTC)
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The UJSM is base on 4 th gen using bakers yeast. Awesomely easy and cheap recipe BTW!
The All Brann is first gen using Distillers yeast. Not yet sold on this one...smells great running final product! Airing out ATM.
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