Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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Well I distilled my first mash today... turned out to be a failure. It was a small batch of 2 gallons and to start it was tainted by silicon that fell into the mash while fermenting. I figured this out when I opened my lid yesterday. It wasn't fully fermented still bubbling a bit. I got rid of all the silicon and used an epoxy this time that gets hard and seems to work great. I ran some of the mash anyway for test runs and had a few problems. I never got a drop of liquid out of the condenser until the temp reached about 200F. I kept the heat low so it slowly raised to 170 in about 10 min maybe bit less in a 1.5qt pot. I tossed the first bit and what I did collect has a pretty strong odor of.. I dunno something about like finger nail polish remover... just not quite as strong. Anyway got another bigger batch of mash started tonight and gonna go from there.. until next time!
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Rank: Senior Member Groups: Registered, Moderator Joined: 4/14/2010(UTC) Posts: 1,666
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Remember this....doing the exact same thing and expecting a different result is the definition of insanity. Follow a recipe and if you followed one last time and it turned out like that use a different recipe. I know we can throw lots of things together and make a wash that will work but if you use something thats tried and true it will not only come out better but it will build your confidence to take another step. Good luck.
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Rank: Guest
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Joined: 2/10/2002(UTC) Posts: 5,254
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Well sorry to hear it didnt turn out as expected. Sounds like you was close. Few minor changes and next time should be better. Originally Posted by: Mkjt88 Well I distilled my first mash today... turned out to be a failure. It was a small batch of 2 gallons and to start it was tainted by silicon that fell into the mash while fermenting. I figured this out when I opened my lid yesterday. It wasn't fully fermented still bubbling a bit. I got rid of all the silicon and used an epoxy this time that gets hard and seems to work great. I ran some of the mash anyway for test runs and had a few problems. I never got a drop of liquid out of the condenser until the temp reached about 200F. I kept the heat low so it slowly raised to 170 in about 10 min maybe bit less in a 1.5qt pot. I tossed the first bit and what I did collect has a pretty strong odor of.. I dunno something about like finger nail polish remover... just not quite as strong. Anyway got another bigger batch of mash started tonight and gonna go from there.. until next time!
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Rank: Senior Member Groups: Registered
Joined: 1/12/2012(UTC) Posts: 804
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Originally Posted by: heeler ... if you use something thats tried and true it will not only come out better but it will build your confidence to take another step. Mkjt88, IMHO the above quote is, hands down, the best advice anyone could ever give. --JB
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Rank: Senior Member Groups: Registered
Joined: 1/27/2012(UTC) Posts: 526
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Hey 88 would you mind telling me what the silicone you've replaced with epoxy is being use for.
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Rank: Senior Member Groups: Registered, Moderator Joined: 7/25/2009(UTC) Posts: 2,209
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Originally Posted by: Bushy Hey 88 would you mind telling me what the silicone you've replaced with epoxy is being use for. DITTO --- I was too lazy to ask.
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Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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The epoxy was to keep my fermenter lid airtight. I have a copper tube coming out of the top of a 5 gal bucket dipping into a bowl of water on the other end. I had junk flex silicon at first and the moisture took it off and it mixed with my mash..
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Rank: Senior Member Groups: Registered, Moderator Joined: 7/25/2009(UTC) Posts: 2,209
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Soo now you have the lid epoxyed on?????
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Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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The lid isn't no. The lid has a rubber gasket and snaps on. I cut a hole in the top of the lid to run my tube through then epoxy is around that.
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Rank: Senior Member Groups: Registered, Moderator Joined: 7/25/2009(UTC) Posts: 2,209
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Originally Posted by: Mkjt88 The lid isn't no. The lid has a rubber gasket and snaps on. I cut a hole in the top of the lid to run my tube through then epoxy is around that. OK SORRY lol lol
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Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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After reading my post I understand why you thought that.. I didn't specify to well
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Rank: Senior Member Groups: Registered, Moderator Joined: 4/14/2010(UTC) Posts: 1,666
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88... ya know a five gallon bucket will work and last virtually forever. And you can do 1-2-3-4 gallon washes in it too. It dosen't have to be a food grade just clean it really well and of course make sure you pick one that wasn't used to store nuclear waste. They all come with a lock down lid with a good seal. I've used the same buckets for beers and likkers and even brandies. I think a bucket is ony 5$ ya know. And a airlock is maybe 3$. Anyway just a thought.
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Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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Ya I got a brand new bucket and washed it first. The airlock is cheap just didn't wanna wait for it to ship so I used the extra tubing I had and it works great now. I slightly changed the ingredients this time.. I used 2.5 lbs of cornmeal 4 lbs of sugar and 4 gal of water.. Does this seem like an ok mix to you guys?
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Rank: Senior Member Groups: Registered
Joined: 1/27/2012(UTC) Posts: 526
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Hey 88 thats going to give you about a 7% wash. With 6Lb you will get about a 10% wash. 8Lb wil give you about a 14% wash. Might want to add a couple more pounds.
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Rank: Guest
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Joined: 2/10/2002(UTC) Posts: 5,254
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Double dittos. Not enough sugar..too much cm for that size batch. Round the meal down to 1.5-2 lbs max 1/3 of a five bound bag give you three nice 4 gal washes. For sugar I try to give a five or six gallon wash 10 lbs with distillers yeast. Might consider 7 or 8 for bread yeast. Somebody just needs to do the math to downsize it one notch:)
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Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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Thanks a lot guys.. Should I pop it open and add he sugar now as its been fermenting all day or add t in a day or two?
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Rank: Guest
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Joined: 2/10/2002(UTC) Posts: 5,254
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Now now now..lol. Longer you wait the more danger which is lurking. Like it overflow and consume us all ect. I just added some rye in mine which I got to clowning around on the compooter and plumb forget. Yeastes is forgiving at least on the front end. Just my .02 of course. Results from ohers may vary.
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Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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Alright well i had maybe just over 2lbs left which i stirred in so now back to the waiting game.
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Rank: Guest
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Joined: 2/10/2002(UTC) Posts: 5,254
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Okay..think you made the right decision Sir. Every little bit helps as the conservation ossifer say as he/she made wee wee in the pristine river. Those guys and gals are dedicated no doubt. I used to know an old Tanker who served with Gen Patton who watched him do it in the Rhine or Rhone...I get them goofy European Rivers mixed up sometimes. All will be well with you and yours..and your hooch. We have a high confidence level.
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Rank: Advanced Member Groups: Registered
Joined: 8/22/2012(UTC) Posts: 201
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Appreciate the help... would be lost if it wasn't for this forum.
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