Please excuse very poor grammar. I'm more concerned with getting the details across at this point than making them sound good. lol Please forgive the formatting too. I copy/pasted this from an email that I sent.
Here are my initial results using the Essential Extractor II with 1100 watt hotplate from Brewhaus.
Using digital Thermometer with sharp point just below final condenser take off.
89C highest temp reached with short column and no cooling flow.
93C with long column.
Using glass lab thermometer placed equal or just below take off.
98C short column.
99C long column.
Turned on cooling water with slightly kinked hoses and temp of lab therm at 99C. Temp dropped to 92C. Distillate of
water increased and then nearly stopped somewhere along the way in a short amount of time.
Switched hoses over to final condenser only and it started dripping water from the condenser tube into the
collection jar very fast at 96C.
Temp stabilized and drip ,almost a stream, remained fast at 98C. Cooling water rose to 27C/80F after 30 minutes or
so.
I can get and keep my cooling water lower as well as increase flow by keeping lines less kinked so I'm not concerned
about that too much yet.
I am questioning my heat and thermometer readings though. The lights on the same breaker as the 1100 watt hot plate
dim some when it is turned on. I currently am not using a diffuser plate but will be adding one later.
Is it possible that My hot plate is not getting hot enough due to low current? Do the above temperature and results seem
normal? Should I see a big change when I add column packing?
It got late on me and I had to quit for the night but I never did get it to output at equilibrium or fair rate in
reflux mode.
Any tips or suggestions that may help narrow the time I spend playing and experimenting to get down to distilling
would be very much appreciated.
Thanks for your time and help,
BTW: Water boils here at 99.4 degrees C
Allen
UPDATE:
A few more details from the next night of playing around while only giving it sporadic attention. ,I was more
preoccupied brewing some beer with a buddy of mine
Still distilling water. Heat on max. Using final condenser only with long column length. No diffuser plate. Cooling
water 21C/70F. Take off temp is 97.5C according to the lab therm. and 99C according to the digital. I lowered the
point of the digital from above post to try and expose more of it's stem to the top vapors. The top of the lab therm
bulb is level with bottom of the output tube to the final condenser and centered in the top. Digital is halfway
between the the lab therm and the opposite side of column from final condenser outlet. Output of water is 148 large
drops per minute or 2.5 per second. Still and cooling water has remained steady at this for the past hour. For
cooling I'm using a cheap thin garden hose wound in a coil around galvanized 3 foot fence wire half submerged in 20
gallons of water and half in the air being blown onto with a fan. Without the fan it will rise to at least 80F but
with it stays at 70F. Still will stop output when switched to reflux mode and not start back with cooling water at
21/70C and several half kinked spots in the cooling lines. Still not using any column packing yet.
1/2 hour later cooling water has risen to 79F and output has slowed to around half? didn't count drops just guessed.
Do I need to be looking at my heat source, cooling source, or current to heating source to improve results?
Next thing on the cooling since I already have the stuff lying around is another hose/fence tower as described above
but with a larger fan blowing up from current tower into new air cooled coils instead of down from top of current
coils toward water as it is now. The fan is strong enough to draw air in around lower coils and water surface and
blow it up through the upper coils. I may have to make up a picture to communicate the cooling structure but later.
That is not important for now. If cooler cooling water is what I need then I can add ice until I get everything else
worked out. Eventually though I would like to avoid wasting ice and or water and do the best that I can with
air/water/fan/coils.
I would like to be able to distill fairly pure water for beer and winemaking. I know I need to add some things back
that get removed but right now I'm more concerned with getting closer to the purity/efficiency point first.
Thanks in advance for any help. I need a lot,
Allen