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#1 Posted : Friday, February 09, 2007 9:50:09 AM(UTC)
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Hey All,
Longtime reader, first time writer here.
I have two 5 gal buckets and a wash recipe that has always worked for me in the past, but now I have 10 gals of seemingly dead wash. My recipe is simple. Into each bucket goes 15 pounds of dextrose into 4 gal of water with two packs of EC-1118 champagne yeast, .5 oz. of citric acid, and 1 0z. of yeast nutrient. I pitch the yeast at 80F at a S.G. of 1.160. All good, but this time nada. The only things I did change was to put .5 oz more of citric acid and put the buckets outside before the airlocks showed any signs of life.
That was three days ago.
Since then I have tried to restart it by: stirring it up, reheating a gallon to bring the whole up in temp, pitching another packet into a gallon of wash ,that didn't go either..., and tossing in four Flintstone's vitamins ,from my forum readings,, but all to no avail.
Halp!
Where does one get potassium nitrate?
Am I missing the reincarnation incantations?
Does one sometimes have to just toss a wash ,a washed out wash?,
Halp!
And really TERRIFIC forum by the way!
Thanks,
PJ Lily
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#2 Posted : Friday, February 09, 2007 12:10:16 PM(UTC)
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PJ, I'm at a total loss also. Offhand, I would say that 15# dextrose is too much for only 4 gal. useing ec1118,and would kill the yeast, but since it has worked for you before??? Plus all the other you have done.

I just made a high gravity rum run ,not as strong as yours with same yeast and with no starter, and after 40 hours, nothing. Frustrated, I pitched a pack of turbo 48, and had to put it into the bathtub and pull the airlock it became so violent. Finished totally dry in 3 days as opposed to just turbo which usually takes a week or longer.

Wish I could help you more, but there are others here more versed than I. I kept mine at 77 deg.
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#3 Posted : Friday, February 09, 2007 5:08:25 PM(UTC)
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Hey John,
Thanks for writing back. You're gonna love this...
So I spoke with the guys at my local brew making shop and they think I may have added too much acid, so they suggested I dilute each bucket with 2 gallons of warm water. This I did, putting the 4 gallons into another bucket. Just for the heck of it I threw in four Flintstone's, some regular yeast nutrient, and 2 packs of EC-1118. And guess what? Yup. When I came back from work the only bucket going was the new one. The original two are still just sitting there doing a whole lot of nothing.
Sigh.
I have already ordered 4 packs of the Turbo 48. With this I should pitch ONLY ONE packet, eh? Especially as I don't have a bathtub! But do you think that after a week and all my trying I should pitch in the Turbo 48 into the two originals? It's not too late?
PJ
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#4 Posted : Saturday, February 10, 2007 1:21:58 AM(UTC)
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PJ:

I'm just curious, why do you use ec 1118? I know it's a bit cheaper than turbo, but after you add all the nutrients, vitamins, and acid is it really worth all that trouble?

I think that diluting and aerating the wash reduced the OG allowing the EC1118 to kick in, but I can't phathom why in only one bucket. Like John I was surprized when you said that the wine yeast had worked in the past with that high of a gravity. However as long as you have sugar for the turbo to eat it should work okay for you.

Me? Sugar is cheap, I'd toss the first two buckets and put my turbo into a fresh wash, but that's, of course, your call. With everything you have invested into this wash it would be interesting to see how the turbo reacts. Please let us know how this works out for you.
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#5 Posted : Saturday, February 10, 2007 3:10:04 AM(UTC)
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PJ

I ditto everything Elricko said, and also with this caution. The turbos have a certain amount of nutrients, balanced for a 25 liter ferment. With all the stuff you have already added to your 4 gal mash, you are going to have way too much. I have read many posts stateing that an overabundance of nutrients, results in very bad and off flavors, oders, and by products. I would either do what you did with the diluted, success, or toss and start over.

And even with the turbo 48, you may want to drop your OG a wee bit, cuz, even though it will probably ferment out, you will get a much cleaner distillate. High Grav. stresses yeast and they will produce more off stuff.
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#6 Posted : Saturday, February 10, 2007 6:12:18 AM(UTC)
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Hey John. Hey Elricko.
Thanks again for writng back.
I've used the EC-1118 because that was what was recommended to me when I was starting out. Until now I've not had much of a problem getting my wash to happen - then again, it is all I've ever used ,don't fix what's not broke, and so don't know the joys of anything else.
I think, adding up what you two guys have told me, that I will bite the bullet dumping the two buckets of wash to start over when my Turbo 48 arrives. Sorry Elricko for not going through with the possible Turbo-fixed wish wash! If I don't it just sounds like it will continue to be a problem into the distilling and tasting.
I'm wanting to nail down the 'simple' sugar-water wash, both for distilling practice and tasting before I venture off to the 17 other recipes I want to try; is there the sure-fire dextrose, water, and Turbo 48 recipe I should use in my two five gallon buckets?
And as always gentlemen, a TERRIFIC forum!
Thanks,
PJ Lily
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#7 Posted : Saturday, February 10, 2007 11:20:39 AM(UTC)
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PJ,

I know it will work fine in your 5 gal. buckets. But, just a thought for long range economics- the turbo's are desighned for a 25 liter, 6.5 gal. batch and 8 kg ,I use 17.5# sugar- a little more if useing dextrose,. If you don't have to move them perhaps use a rubbermaid trash can with lid, and do two batches at once, 13 gal. at once? or 3- 5 gal. buckets with 2 full batches divied up between them. Just a thought.
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#8 Posted : Saturday, February 10, 2007 3:36:25 PM(UTC)
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John,
Wow! Thanks! I would have blown it for sure without your advice ,but assuredly come out with a fantastic story of woe, about the Turbo yeast. Three buckets it is then.
So into each bucket would be ,not in order of course, 2/3 packet of Turbo, say 13# dextrose, and water, filling up the bucket to five gal.? 13# of dextrose is not that much less than the 15# I was using previously...
Are carboys 6.5 gallons and if so should I just bite the bullet and buy two; my boiler is a 13+ gallon keg. If so then I could buy that stick-on thermometer for the carboys that I saw and coveted at the beer making shop,!,
After a number of successful tries with this recipe what would you suggest be a sensible next recipe? There is a poteen recipe on the recipe forum that has peaked my interest...
Thanks again,
PJ Lily
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#9 Posted : Saturday, February 10, 2007 5:19:00 PM(UTC)
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PJ,

If i may join the thread here, i believe a good method would be making the 'double-batch' of 6.5 gal turbo 48 in the same container ,double water amounts, double sugar amounts, and double yeast - two packets, and when ur ready to set them aside, that's when i would split them into the three separate buckets. i think that would be a lot easier than trying to measure thirds of yeast packets etc etc... maybe not though.

Good luck!

Rob
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#10 Posted : Saturday, February 10, 2007 6:56:55 PM(UTC)
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Robert expresses and explains it better than I did. Mix it all together, and split into smaller carboys. What also might be good is to let the initial ferment subside,and then split into the 3 carboys. Any of them would work well I think, but the best would just allow the whole batch ferment as one entity, and distill or strip it all quickly. ie, the garbage can, Or like Robert said, disperse into seperate smaller fermentaters.
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#11 Posted : Saturday, February 10, 2007 7:29:50 PM(UTC)
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PJ,

If like you said you are planning going forth, and continueing into quality flavors ,not that vodka isn't, then i would whole-heartedly suggest you invest in 25 l or 6.5 gal. fermentaters. Most all recipies, and products, such as turbo's, are designed and geared for this.

As an additional aside, once past the vodka stage, you will want to do several stripping runs, at least 3, before a spirit run, and then you will want to acrue a sizeable amount before ageing. There are cheap alternatives, and somewhat better, if you don't want to wait years.
Accumalate 5 or 6.5 gal. jugs or buy new, they are cheap. In the meantime, as I do, take your Vodka, or neutral grain spirits, cut to 55% or less and put into your 6.5 gal. or smaller glass carboy with a couple of cups of washed, prepared activated carbon. leave a gallon of airspace and swirle when handy. Just leave it sit until you need a certain amount, and carfully pour off. Filter through a coffe filter ,I use an eight inch dia. ss fine screen colander or large tea filter looking thing.

cut to whatever proof you want to bottle at and add add least a tsp of glycerine ,is really cheap and makes a dramatic differende,.

assertain and appraise your long term goals. Aside from vodka, you will have to cure and store your spirits for a period of time.

Organize and plan, and utilize now cheap resoarces, that you will be able to utilize later.

And after all that, make an excuse for why I can't use words properly- that wasn't a sassafras leaf- scratch, sctatch, itch, ith- I already used up my dictionary.
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#12 Posted : Sunday, February 11, 2007 2:51:02 AM(UTC)
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PJ:

John is giving you good advice. As far as fermenting buckets, I use three 8.5 gallon buckets that are available from either brewhaus, mile-hi or most homebrew shops. The usually run about $18. When I make a double batch, I use two buckets and pitch two packs of turbo. Once that's done I pour bucket one into the third bucket and put in clearifier, then I wash the emptied bucket. Then I pour the second wash into the first bucket and add clearifier. Kind of like rashing rings these are a one time cost and worth it because as john says, everything is geared for 25L batches. This will give you 13 gallons of wash which is perfect for a keg.

Now as far as longer time storage of distillate, I use glass. If you want to accumulate like John is talking about a glass carboy is the way to go. This is aside from your fermenting buckets.
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#13 Posted : Sunday, February 11, 2007 12:03:47 PM(UTC)
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Hey John, Elricko, and Robert,
Gee, shoulda been a long time writer a long time ago...
Some clarifying questions and then a recipe/method formula:
Elricko: do you really mean 'pour' or do you mean rack ,siphon, the wash from one bucket to another?
All: when would I want to use a glass carboy over a plastic bucket?
All: is sparkleoid the clarifier y'all use?
All: is there a post which thoroughly explains a stripping run so y'all don't have to repeat yourselves ad nauseum?
And so a good recipe and method could be:
boil 4 gallons of water
add 10# of dextrose
cool to 75F to 80F in a 8.5 bucket
pitch the Turbo 48
wait the 48 hours
boil and add one gallon of water with 3# of dextrose
wait another 48 hours
rack off to a clean bucket
add clarifier
wait another 24 hours
rack off into boiler
distil and age to taste with art and patience
drink
I would like to have a series of wash to distil successes in terms of regular amounts and taste before I branch out to to more comples recipes and reflux adjustments. Could the above be the ticket, ya think?
I really appreciate your time.
Thanks guys,
PJ Lily

Hi Aidan! ,the six year old wanted to see his name on the screen,
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#14 Posted : Sunday, February 11, 2007 12:14:56 PM(UTC)
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Oh ya,
My favorite new John word is Fermintator!
My gal wanted to know if that would be an all potato mash? I told her, 'ya, duh.' Girls. LOL
Keep up the good work!
PJ Lily
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#15 Posted : Sunday, February 11, 2007 12:43:08 PM(UTC)
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PJ,
I don tole ya, best watch where yer step. Dun used up my dictionary in or hind the outhouse. Careful them pison ivee leaf also. Make you scratch yer Fermintator!

Cross eyed, tongue tied, too fingered typist!
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#16 Posted : Sunday, February 11, 2007 1:42:54 PM(UTC)
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I'll let some other mor knowledgable people answer some of your questions.

I use sparkaloid with fantastic results. I set my wort outside in the cold overnight, bring in, and add the sparkaloid, and keep room temp. 24 hours at most. I notice that after so many hours there are conglomerants ,remember, I l used up my dictionary, floating from the middle or so down. I will knock on the sides like on a house door, and almost immediatly, they begin to drop.

In over 50 sugar washes, i have never had a problem. I put 17.5# sugar in fermentater, run the bath tub till its hot, shove fermentater under faucet, and stir till about 15L. stir till dissolved, let rest and stir again, agitating as much as possible to aereat. Add cool water to bring temp. to pitching temp. Pitch turbo, cap and seal with airlock. Has never failed me.

If you are going to the trouble of boiling, why not use cane sugar and a little acid to make dextrose. Invert sugar. A lot cheaper if you are going to boil anyhow. Correct me if I am wrong.

With the turbo 48 I add all sugar, 17.5# at beginning and no problems. Put into spare bathroom and keep at 75 deg.

With turbo's its so dang simple, easier than typing all these strange words.
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#17 Posted : Sunday, February 11, 2007 2:20:38 PM(UTC)
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John,
Thanks for the quick return. General George S. Patton once said 'any damn fool could write a word the same way all the time, true genius was writing it different every time.' His advice and yours I look to often.
Coupla questions ,again,. What is your final volume amount with your 17.5# sugar wash. I know you're adding 15L, but how much cool water do you end up adding to get what final volume.
The other question is if you have a a ratio of acid to cane sugar and what do you mean by 'invert sugar'? And it will be a LONG time before I am able to correct anyone!
Again, thanks for your time.
PJ Lily
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#18 Posted : Sunday, February 11, 2007 2:57:01 PM(UTC)
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using turbo yeast, a total volume of 25L is the goal ,after sugar, hot water, yeast, cold water,.
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#19 Posted : Sunday, February 11, 2007 3:01:37 PM(UTC)
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PJ, I actually remember that quote also. What a great general he was.

25L total volume, if i read your question right.

I will try my best, to invert sucrose to dextrose, boil sugar water mix with half cup or so of lemon juice, or other acids for about 15 minutes. Supposebly, makes for a quicker yeast kick off, and quicker finish. I've never done it, but just from what I've read, and as youv'e already noticed, the angels keep geeting their share of my memory.

If useing turbo, you don't have to worry about PH as they contain a buffering agent.

Seems like you are an inquisative, and fast learner, and us old farts will have to have someone to remind us of how to do the job right.
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#20 Posted : Sunday, February 11, 2007 3:44:04 PM(UTC)
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PJ:

I meant siphon, sorry about that. Okay, here's my two cents ,or 2 shillings as the case may be,

Here's how I make a simple sugar wash:

Turn on my hot water and let it run until it gets fully hot, then run two gallons ,through a filter, into my 'fermentator'. To that I usually add 16 pounds ,17.26KG, of cane sugar to the hot water and stir until it is all dissolved. I then run cold water through the filter bringing the total volume to 6.5 gallons ,25L,. I check to make sure the temp is below 70 degrees ,21C,, then pitch the yeast ,Mile-hi Turbo48,stirring constantly for about two minutes until it is completely disolved. Next I drop the hydrometer in and get the OG ,usually 1.10,. I then cover, set the air lock and put it in a location where the temp stays around 68 degrees ,20C, for seven days.

At the end of the week I take a second hydrometer reading to make sure it is finished working and then siphon it into a clean 'fermentator' put in SuperKleer ,I like sparkiloid as well, but usually use SuperKleer, then I set it aside again for another three days.

At that point it is water clear and I siphon it off into my boiler and distill. If I have any tails from the last batch I toss that into the boiler as well. I distill using the reflux method. From that I usually get three and a half to four quarts ,4.5L, of 93 to 95% distillate.

That's all there is to it. I know, some of you are asking why I leave it so long in the 'fermentator' and why wait so long to clerify. Hey, I'm just not in that big of a hurry. I let nature take it's course and shoot for the cleanest and maximum yield. I also let it reflux for hours. Again, I'm in no hurry. If I could just slow down the drinking part then I'd really be doing good!

I hopes this helps PJ. Everybody has their own method and their own way of doing things. That's what makes this an art. I look forward to hearing about yours.

Cheers
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