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Offline sunni  
#1 Posted : Friday, December 04, 2009 2:01:39 PM(UTC)
sunni


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"hi all- I am hoping someone can help. We have been having a problem with our last few runs- bad smell and taste (very yeasty and doughy). We are using copper and charcoal. We are making two runs at one time to save time and energy. The temp is holding pretty steady between 78-79. Water temp seem to also stay cool enough. We have noticed that the alcohol content is not as high as it used to be either. We are using 24HR Turbo.

Any ideas? I don't want this next batch to turn out like the last. I have had to refilter a second time. Are we asking too much from one batch of charcoal?

Thanks Sunni"
Offline mtnwalker2  
#2 Posted : Friday, December 04, 2009 5:00:04 PM(UTC)
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"First, callibrate your thermometers for you elev. Boiling water will give you a basis. then adjust your reflux accordingly. Temps you posted seem a bit high. Lower it with coolant water flow. If too slow, add heat to the pot., but keep reflux active. Collect heads slow, then hearts fast, and tails, no coolant and as fast as condensor can handle.

wha fun."
Offline mtnwalker2  
#3 Posted : Friday, December 04, 2009 5:07:51 PM(UTC)
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Put into a glass carbouy with lots of carbon. Let air with a coffee filter, and then check in a few weeks. Will make a dramtiic diff.
Offline mtnwalker2  
#4 Posted : Friday, December 04, 2009 5:42:04 PM(UTC)
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"Giving a bit more thought, are you alllowing your wash to settle? Really clear and clean. I also didn't have a decent stillage, till I insulated the column. Made a vast difference. From that point on, cuts made the difference.

Carbon in the carbouys is fantastic for neutral."
Offline Eekamouse  
#5 Posted : Tuesday, October 12, 2010 7:51:26 AM(UTC)
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"Hello everyone. I have been busy with runs most of this week, and have been happy with my setup. The mash has fermented in proper time, and smells good at .000 final gravity, with a crisp, dry taste. My brewhaus column still is running smoothly, and I am becoming more in-tune with that acrid, chemical fruitiness of the heads and the stale, cardboardy smell of the tails coming on. My temp, at low (5-6%) abv's, is around the mid 180's to low 190's for hearts. Seems a little high, but it runs well and stays consistent.

However, although my hearts runs (on whisky and rum at around 130 proof)) have smelled palatable enough, I find that the taste has a sort of metallic, rubbery quality to it. The first run of whisky had it, and it has softened with aging, but I wanted to ask if this is a somewhat common profile of the taste of fresh distillation, or if it is something I need to fix.

I considered
A) that the rubber bung seal (from brewhaus) at the column top was creating a distinct rubberiness. I can smell it fairly strongly at the column top after a distillation, but then again my nose is right against it! My last run I covered it in foil, and it seemed to help a bit.

B) the loose packed copper mesh bought fom brewhaus was a factor. Towards the base, it comes out a gunmetal colored mixed wit the copper orange.

I know it's difficult to assess such a subjective thing, but I am hesitant to do another run without at least running it by you professionals.

My best explanation of the taste is (drinking whiskey at 80 proof) one of a good starting flavor, with a slightly lingering middle taste of rubber and paper, similar to when you drink water that has been sitting for a while in a paper cup. The finish is fruitier and cleaner, but there is that unpalatable taste right there in the middle.

I am fairly picky about my cuts (although not so experienced yet) especially with tails. I toss even a hint of tails in with the feints. I don't like that stale smoked smell.

Does this ring a bell to anyone?
I would greatly appreciate any feedback on this issue, as I am afraid to go on with another run for fear of wasting my precious ingredients!

Thank you"
Offline Eekamouse  
#6 Posted : Tuesday, October 12, 2010 8:16:41 AM(UTC)
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"Hello everyone. I have been busy with runs most of this week, and have been happy with my setup. The mash has fermented in proper time, and smells good at .000 final gravity, with a crisp, dry taste. My brewhaus column still is running smoothly, and I am becoming more in-tune with that acrid, chemical fruitiness of the heads and the stale, cardboardy smell of the tails coming on. My temp, at low (5-6%) abv's, is around the mid 180's to low 190's for hearts. Seems a little high, but it runs well and stays consistent.

However, although my hearts runs (on whisky and rum at around 130 proof)) have smelled palatable enough, I find that the taste has a sort of metallic, rubbery quality to it. The first run of whisky had it, and it has softened with aging, but I wanted to ask if this is a somewhat common profile of the taste of fresh distillation, or if it is something I need to fix.

I considered
A) that the rubber bung seal (from brewhaus) at the column top was creating a distinct rubberiness. I can smell it fairly strongly at the column top after a distillation, but then again my nose is right against it! My last run I covered it in foil, and it seemed to help a bit.

B) the loose packed copper mesh bought fom brewhaus was a factor. Towards the base, it comes out a gunmetal colored mixed wit the copper orange.

I know it's difficult to assess such a subjective thing, but I am hesitant to do another run without at least running it by you professionals.

My best explanation of the taste is (drinking whiskey at 80 proof) one of a good starting flavor, with a slightly lingering middle taste of rubber and paper, similar to when you drink water that has been sitting for a while in a paper cup. The finish is fruitier and cleaner, but there is that unpalatable taste right there in the middle.

I am fairly picky about my cuts (although not so experienced yet) especially with tails. I toss even a hint of tails in with the feints. I don't like that stale smoked smell.

Does this ring a bell to anyone?
I would greatly appreciate any feedback on this issue, as I am afraid to go on with another run for fear of wasting my precious ingredients!

Thank you"
Offline mtnwalker2  
#7 Posted : Tuesday, October 12, 2010 9:36:34 AM(UTC)
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"Sounds like you are getting your column pucked in or foam comeing up. Especially rums are bad for this. Some vegetable oil, butter or anti foam agent helps with this. If that happens you can get all kinds of bad tastes and smells.

But if you are running whiskey and rums why are you not pot stilling? No packing and just the top half of the column. Although I do use one coil at the very top to react to any sulfer. Also, best to do several stripping runs and then a combined spirit run. Some whiskeys like Irish are even tripple distilled.

Never noticed a rubbery tast or smell form mine, and I never tried smelling the bung close up while hot.

Back flushing the column with a gal of boiling water will remove most of the bad smells of tails. Add a cup of vinegar to the water and boil it if you want. Generally the foreshots and heads from the next run will clean it out also."
Offline Eekamouse  
#8 Posted : Tuesday, October 12, 2010 10:07:18 AM(UTC)
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"To clarify, I have the brewhaus column potstill. That was confusing on my part. I wouldn't think that I would be getting fluid in the column. I use a 7.5 gallon keg that I usually only fill to around 4.5 gallons at most. But that would explain several things, including the high temps. I'll give the anti-foaming stuff a try.

Thanks, Mr. Mountain"
Offline mtnwalker2  
#9 Posted : Tuesday, October 12, 2010 11:02:43 AM(UTC)
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"Another issue, the smaller the batch being run the harder to make good quality cuts, esp. running a pot still. I get much better results running 50L in a keg, then I do running 25L in the 7.5 gal pot. 17 or 18 L runs are going to be tough for you. Defininetly do stripping runs and combine several for a good spirit run. Then if still not the quality you want, do a third run.

PS. When doing rum runs (not sure this would work for a small run) when you hit the tails, at whatever point you want to toss to feints, keep running till lower down ABV feints. There is an acid that comes over that if added to the rum greatly increases flavor and quality. Same acid I believe, that the mountaineers used to collect as yellow jacket bee piss. OAM, so can't remember the name of the acid. They used it to make confectionaries and also to rub on arthritic joints for relief. Simple to collect in the fall of the year.

Cheers!



Originally Posted by: Eekamouse Go to Quoted Post
To clarify, I have the brewhaus column potstill. That was confusing on my part. I wouldn't think that I would be getting fluid in the column. I use a 7.5 gallon keg that I usually only fill to around 4.5 gallons at most. But that would explain several things, including the high temps. I'll give the anti-foaming stuff a try.

Thanks, Mr. Mountain
"
Offline LWTCS  
#10 Posted : Tuesday, October 12, 2010 12:28:20 PM(UTC)
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"Sunni.
Get yerself a better recipe.
Keep your ABV below 14%.
Let it clear very well after it ferments.
Strip run. Dilute to 35-40% and spirit run.
Collect in small jars.
Let your distillate air for at least a day.

At the cutting bench start wi"
Offline scotty  
#11 Posted : Tuesday, October 12, 2010 12:35:50 PM(UTC)
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:)I never get any rubbery smell from those bungs--they have beem perfected for years:)
Offline Eekamouse  
#12 Posted : Tuesday, October 12, 2010 4:21:17 PM(UTC)
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"It would seem that the strip run is what I need. Sounds like my bung and copper aren't the problem. I checked, and I definitely don't have a foaming problem.
Here is my info for a UJSM mash..
I use the brewhaus pot still column, with a loosely packed (I can see plenty of light through the tube) amount of copper scrubbers from the base of the column to right before the arm. I usually run around 4.5 gallons at around 5-6% abv for the whisky. I use a propane turkey frying burner with a thick metal plate placed between the direct flame and my 7.5 gallon keg (for scorching). In the end I get around a quart of hearts at around 135 proof. For my last few runs, the hearts seem to be peaking around 186 F. I would say I get about 150 ml every 15-20 minutes. In total I get 3 quarts on average (without running tails below 100 proof).
I insulate the column with doubled over cotton towels (cheap mans insulation) as well as the top of the keg. I am sure some part of my process must be way off.

Well, with all of that info, I guess my real question is.....should the distillate taste fairly good right out of the still? Because mine does not. It has a stale, papery flavor, although the smell is pleasant and corny.....should I just be running it again? And if so, is a few quarts of distillate in a 7.5 gallon keg enough to run again, or should I add water?

I am asking too many questions. I am letting myself get frustrated, but I want to wrangle this darned pot still!"
Offline Eekamouse  
#13 Posted : Tuesday, October 12, 2010 4:27:37 PM(UTC)
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"[PHP]Let it clear very well after it ferments.
Strip run. Dilute to 35-40% and spirit run.
Collect in small jars.
[/PHP]

I see part of my question about adding water to my post-strip distillate was already pointed out.

My mistake!

Thanks"
Offline scotty  
#14 Posted : Tuesday, October 12, 2010 4:47:01 PM(UTC)
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"
Originally Posted by: Eekamouse Go to Quoted Post
[PHP]Let it clear very well after it ferments.
Strip run. Dilute to 35-40% and spirit run.
Collect in small jars.
[/PHP]

I see part of my question about adding water to my post-strip distillate was already pointed out.

My mistake!

Thanks



:) I hear lots of folks say negative things about turbos. I never used anything except ec1118 for wine or mash .

:)All i'm asking is if that yeast that says 24 hour turbo or whatever is not part of the problem. it seems way too fast to be good-- in wine makeig,the secret to getting great results is slow and easy with all stages of th process.

I know nothing about turbos though"
Offline mtnwalker2  
#15 Posted : Wednesday, October 13, 2010 3:09:29 AM(UTC)
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"Sounds like either your vineometer or alchometer is off. If you are running 18 quarts of a 6% wash, you only have 1.08 qts of potential alchohol to capture and you are leaveing a lot behind cutting off the tails at 50%.

Harvesting a full qt at 135 proof sounds like you are getting a good bit of heads in there.

Strip a good few runs, then dilute and run slow with tight cuts. Save the feints for a later run when you have enough. The more you dilute, the less flavor your final whiskey will have though.


Originally Posted by: Eekamouse Go to Quoted Post
It would seem that the strip run is what I need. Sounds like my bung and copper aren't the problem. I checked, and I definitely don't have a foaming problem.
Here is my info for a UJSM mash..
I use the brewhaus pot still column, with a loosely packed (I can see plenty of light through the tube) amount of copper scrubbers from the base of the column to right before the arm. I usually run around 4.5 gallons at around 5-6% abv for the whisky. I use a propane turkey frying burner with a thick metal plate placed between the direct flame and my 7.5 gallon keg (for scorching). In the end I get around a quart of hearts at around 135 proof. For my last few runs, the hearts seem to be peaking around 186 F. I would say I get about 150 ml every 15-20 minutes. In total I get 3 quarts on average (without running tails below 100 proof).
I insulate the column with doubled over cotton towels (cheap mans insulation) as well as the top of the keg. I am sure some part of my process must be way off.

Well, with all of that info, I guess my real question is.....should the distillate taste fairly good right out of the still? Because mine does not. It has a stale, papery flavor, although the smell is pleasant and corny.....should I just be running it again? And if so, is a few quarts of distillate in a 7.5 gallon keg enough to run again, or should I add water?

I am asking too many questions. I am letting myself get frustrated, but I want to wrangle this darned pot still!
"
Offline Eekamouse  
#16 Posted : Friday, October 15, 2010 9:37:48 PM(UTC)
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"Wellllll, to figure out my strange rubber/paper taste problem, I thoroughly cleaned my distilling keg, along with all parts, and boiled distilled water through the setup (minus the keg seal O-ring and rubber top seal).

I found that my rubber keg seal was most definitely imparting a taste, as well as the rubber top.
However, the very first run I made with the column ( an all grain rye) scorched big-time, and tainted everything it touched. So it's my fault, not the parts.

I thought I should mention this, because even after several cleanings with vinegar, soap, you-name-it, the smell never left the rubber. My greenhorn mistake still haunts me! So if anyone else has had a similar mishap, I would suggest thinking twice, or at least thoroughly smell-checking any parts, before using them on another run.

On another note, I found that my copper mesh was creating an off-flavor as well. It's pure copper, so I was wondering if anyone thought it could be my water source. It is limestone aquifer water, so it has a relatively high alkalinity.

Thank you"
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