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Offline Tracyman0111  
#1 Posted : Wednesday, November 28, 2012 4:35:11 AM(UTC)
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"First off, as a novice to forums as well as distilling, I apologize ahead of time if there is another section where this post would be better suited; I spent some time looking, but didnt see a closely related topic.

Ill try to be as detailed as possible with every aspect of my process, so you guys can help me look for any errors. To start, I am using a 7 gallon Brewhaus stainless steel column still. Cooling is done with a mini sump pump dropped in a 4 gallon stock pot of ice water. There is a ball valve in the cooling hoses, which I keep fully open all of the time. Secondly, The only mashes I have experimented with so far have been very simple, even down to sugar water yeast.....I have had the same issue with every mash, which makes me think my problem lies in my still operation.

5 gals water, boiled and added 10 lbs of sugar. Let cool to around 75F, add a tablespoon of yeast. Its generally taken approx 5 days for fermentation to cease, and I gauge that off of when it stops bubbling. I fill and heat the still, takes about an hour or so to come to temp, but I back down the heat, turn on the water pump, and start regulating temp at around 175.

As distillate begins to flow, I try and separate out about 1.5 inches in each jar, for testing purposes. The majority of the product Ive gotten out is clear, burns blue with minimal bubbles, and runs around 155-160 proof. Problem is, it smells and tastes HORRIBLE, almost like spoiled food.

One of the major questions I have---my thermometer is all the way at the top of the column, with nothing on the kettle itself. Im wondering if, by running off of the temp reading in the top of the column, Im actually running overtemp in the kettle? But on the other hand, if that was the case, wouldnt it have been designed with a thermo in the kettle? Again, I BEG for any opinions, but I feel like the problem lies in my operation, not the mash recipe. I look forward to hearing from you guys!!!

Travis"
Offline ohyeahyeah  
#2 Posted : Wednesday, November 28, 2012 10:26:29 AM(UTC)
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I'm pretty sure Rick will add a bung for a thermo in the kettle if you request it when ordering. But with a reflux still the temp at the top of the column is more important then the temp at the boiler.

Are you saying you are running full cooling to the tower the entire run? I don't run one of these setups but my understanding is that you should only be running full coolant to the tower during the first stage of full reflux until you reach equilibrium which takes about a half hour. So i think you are running with too much heat. Also your still should produce around 92% alcohol and any lower is an indication you are running too hard.

Describing how you run your still would be helpful. I don't think a 4 gallon pot cuts it as a coolant tank but i guess as long as you keep replinishing the ice it could work.

Maybe someone could relay how they use their brewhaus still.

What i would do is run it like you seem to be and as soon as you see product cut your heat back until you no longer are getting product out. Note the temp for future runs. Leave it like that for a half hour(full reflux). Then turn down the coolant flow to the tower until you start to get product out the condensor again. Toss the foreshot and collect like you are in small increments checking the abv. If your abv is lower then 92% turn the flow to your column back up in small increments until you are reaching that number. Continue to collect in small increments keeping jars in order. Once your column temp starts to climb and your abv is dropping your are into the tails. At that point you can either shut down or if you want to collect tails you can turn off all coolant flow to the tower and run the tails fast. Cover your product to keep out dust, dirt and bugs with something breathable like paper towel and leave over night. Smell test and if you like taste test jars to pick keepers.

My 2 cents.
Offline Bushy  
#3 Posted : Wednesday, November 28, 2012 11:41:08 AM(UTC)
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Hi Tracyman, Take a look at the thread called "Yesterdays Run" on the second page of the "GENERAL" section. It describes one of my runs.
Offline Bushy  
#4 Posted : Wednesday, November 28, 2012 5:14:13 PM(UTC)
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Hey Tracyman are you letting the solids settle out a few days after fermentation stops before racking your cleared mash off the traub on the bottom, or are you just throwing the whole thing in the boiler?
Offline Tracyman0111  
#5 Posted : Friday, November 30, 2012 3:23:19 AM(UTC)
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ohyeayea--thanks for your description of the run process, sounds like theres definitely some worth trying there. A fella on another forum also told me theres no need for ice, what gives?? I cant see that being true, as a closed cooling sysytem will eve
Offline Tracyman0111  
#6 Posted : Friday, November 30, 2012 3:33:45 AM(UTC)
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Originally Posted by: Bushy Go to Quoted Post
Hi Tracyman, Take a look at the thread called "Yesterdays Run" on the second page of the "GENERAL" section. It describes one of my runs.



I understand I have a lot to learn, seems there are a lot of numbers and calculations and such. I have kind of been hoping there was just a plain old simple wash I could run to learn with, all the ingredients dumped in the wash at once.

Heres how I make my wash---i take about 4 gallons of h2o, bring to a rolling boil, dump in my sugar, continue to heat and stir until all sugar is melted. I let cool down to room temp, add a tablespoon or so of standard generic brewers yeast, bought from the local distiller supply. I gently stir in the yeast, and let sit, covered with a towel, INDOORS, until all the bubbling stops, which has generally been anywhere from 3 1/2 to 5 days. I then pour into kettle and proceed with my run as described in my first post.
Offline John Barleycorn  
#7 Posted : Friday, November 30, 2012 4:33:40 AM(UTC)
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"Hi Tracy,

Just a few quick questions: When you say it tastes ""horrible"" are you referring to each and every individual jar you collect? Or are you combining them and tasting the mix? Also, are you diluting before drinking?

Read that post bushy mentions, it has a LOT of excellent information all in one place ... especially about equalizing and power adjustments.

As far as temperatures go ... IMHO a thermometer gives you nothing more than ballpark numbers. And having one at the kettle offers you almost nothing when using your column. I still use one, but it's only because I need something to plug the little hole in the bung. The fact that I can look at it from time to time to get a feel for where I am in the run is handy ... but my adjustments are never based on temps.

Here's a Reader's Digest version of how I run my rig (PSII HC, 1500w) ...

Warm up at full power, no column cooling. I'm a ninny about uncontrolled vapor so I ALWAYS have cooling to the product condenser. Once the fores come across I start reducing power (still no column water). Once heads start I back off the power to a slow drip, then go full reflux for at least 40 minutes (full column water). Then I back off the column cooling and collect heads very slowly. Once into hearts I may have to bump up the power slightly. If I increase power, I always go full reflux again for at least 15 minutes. I collect hearts somewhere around 800 mL/hour ... plus or minus a few hundred mL ... depending on what's in the boiler or what I'm trying to acoomplish ... or sometimes just depending on my mood. BigGrin

Nothing I do requires a thermometer. All of my adjustments are based on two simple things: (1) control your collection rate and (2) control how hard you drive your column ... that's all. Collection rate is pretty obvious ... it affects the reflux ratio. Trying to avoid driving your column too hard isn't always as obvious ... especially if you're chasing temps that you read from above the column condenser. But think of it this way: if you put too much energy in you won't get good separation -- you'll just end up pushing everything further up the column ... basically you'll end up with high abv smearing. You'll notice in bushy's description that he's only using enough power to support he collection rate he wants. He's not damning the torpedoes, full speed ahead.

Anyway, I hope this helps.

--JB"
Offline Tracyman0111  
#8 Posted : Friday, November 30, 2012 5:13:42 AM(UTC)
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John--

First off, thanks so much for the time taken to reply and help me out, its greatly appreciated!!

And yes, I am referring to each individual jar, And I have never tried combining. A few runs I have made have produced some cloudy distillate, I figure thats a result of running too hot?

On the temp topic....I have read some posts where guys talk about NOTHiNG but temps, Im assuming this is simply a matter of personal preference and skill level?

One area where I think Ive been going wrong---I never realized that a long delay in distillate production was to be expected and is somewhat of a sign of fractioning? Ive run my still for around an hour or so at full power before I ever saw drips. When that happens I back power down to around 175, but most instances the distillate stops completely about 20-30 minutes later. I didnt know to expect this delay, so at that point I figure Im doing something wrong, and just shut down completely. Now its looking like Ive wasted a lot of wash doing that Cursing

Also, I pretty much run my cooling system full blast the entire time, yet another area I will experiment with changes!! From the sounds of your run descriptions, it sounds like you have 2 separate cooling systems on your rig?? You mentioned column cooling and condenser cooling......i have that as well (my condensor is a metal tube sticking sideways and down out of the top of column, before turning into the rubber hose), but I have no way to separate water flow to each, only a ball valve to regulate flow AMOUNT.

Travis
Offline John Barleycorn  
#9 Posted : Friday, November 30, 2012 6:41:54 AM(UTC)
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"
Quote:
A few runs I have made have produced some cloudy distillate,
Thar's probably from tails.

Quote:
On the temp topic....I have read some posts where guys talk about NOTHiNG but temps, Im assuming this is simply a matter of personal preference and skill level?
Well ... that depends on whether or not you believe that you can truly control the temperature. I don't buy the concept at all. The temperature is going to be what it wants to be. Look at it this way, once you charge your boiler there are only two things you can adjust: your power level and the flow of water to your column condenser. So you can only control (within limits) the latent heat you put into the system (power) and the latent heat you remove (water flow to the condenser). That's all. Everything else will be what the laws of physics say it will be at a given vapor pressure.

Does this make sense? You only have two knobs to turn (power and water). Use reasonable power for good separation (avoid smearing) and manage your reflux ratio ... the temperature should be irrelevant. Just give it try on an upcoming run ... see if it fits your style.:)

Quote:
Ive run my still for around an hour or so at full power before I ever saw drips.
It takes me around two hours to get some output on stripping runs (22L
10% - 12%).

Quote:
When that happens I back power down to around 175, but most instances the distillate stops completely about 20-30 minutes later.
If there's more EtOH available to collect, there are only two things you can do: increase power and/or reduce cooling water to the column.

Quote:
Also, I pretty much run my cooling system full blast the entire time, yet another area I will experiment with changes!! From the sounds of your run descriptions, it sounds like you have 2 separate cooling systems on your rig??
I use one pump and one ball valve. The ball valve controls the flow into the column condenser. I have no way (or need) to control flow into the product condenser.


Quote:
but I have no way to separate water flow to each, only a ball valve to regulate flow AMOUNT.
Ahhh ... you need to move that valve. Put it after the supply side tee (between the tee and the column condenser input). Then you will be able to control the water flow to the column only. The product condenser will be on autopilot.

--JB"
Offline Tracyman0111  
#10 Posted : Friday, November 30, 2012 8:16:42 AM(UTC)
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Awesome info on relocation of the ball valve!! As far as the cloudy stuff being tails, I dont think thats it, as it was the last stuff I collected out of probably a quart, separated in different containers......i should get at least a quart of hearts in itself, out of a 6 gallon wash, right??
Offline John Barleycorn  
#11 Posted : Friday, November 30, 2012 8:42:14 AM(UTC)
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"Travis,

If the abv of your wash was lower than you expected, you may very well have been into the tails ... which would explain why you only collect so much, then saw things come to a halt. The fact that it was the last sample you collected might be a smoking gun.

Did you take original/final gravity readings? If so, what were they?

--JB"
Offline BamaDave  
#12 Posted : Sunday, December 02, 2012 3:36:03 PM(UTC)
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"Travis,

Running the numbers, if you have 5 gallons of water and 10 lbs of sugar your wash should fall in around 1.086 SG. That would yield a maximum of 13% in ~ 6 gallons of wash. That should put you in ~ 3 quarts of 75%(150-160 proof) distillate. That is if everything is absolutely optimal. I doubt you are fermenting to optimal level because you didn't mention any yeast nutrient and my understand is you need this when running sugar washes. In my short time distilling my guess is even under optimal conditions you may get 1 quart somewhat hearts. Remember though, if you are getting 75% alcohol then that is still 25% of something else. That something else is what is likely what is causing your taste. You said it was cloudy, I agree with John, that is definitely tails there. I have never run sugar washes but from reading other posts on the subject they tend to contain large amounts of tails.

What does your wash smell like before going in?

My simple suggestion, combine everything you have run so far that tastes horrible, take a measurement and add enough water to dilute back to ~ 15%. Run this and see if it cleans up. My guess is, it will clean up pretty good. It has worked for me anyways."
Offline ratflinger  
#13 Posted : Saturday, December 08, 2012 4:06:39 PM(UTC)
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If you are wanting a neutral then you are only completing half the process. You should strip in pot mode & then reflux for your final. If you only have a pot stil thi it is possible to a quality product, but you need to distill it more than once.
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